Preparation of High Purity Anhydrous Indium Trichloride 高纯无水三氯化铟的制备
In this paper, the anhydrous indium trichloride was prepared by azeotropic drying. 本文采用共沸去水法制备无水三氯化铟。
With a suit ratio, Indium trichloride and resorcinol dissolve absolutely into the solution of formamide water solution. The reactants were transformed into 22 ml teflon-sealed autoclave and heated at 160 ℃ for some hours. 按照一定的配比,将氯化铟和间苯二酚完全溶解于甲酰胺的水溶液中,然后转入聚四氟乙烯高压反应釜中,密封后在160℃下水热反应一定时间,即得到氢氧化铟中空球。